Multiple Routes of Pesticide Exposure for Honey Bees Living Near Agricultural Fields
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{"title"=>"Fast and easy multiresidue method employing acetonitrile extraction/partitioning and \"dispersive solid-phase extraction\" for the determination of pesticide residues in produce", "type"=>"journal", "authors"=>[{"first_name"=>"Michelangelo", "last_name"=>"Anastassiades", "scopus_author_id"=>"6602758847"}, {"first_name"=>"Steven J.", "last_name"=>"Lehotay", "scopus_author_id"=>"7004838746"}, {"first_name"=>"Darinka", "last_name"=>"Štajnbaher", "scopus_author_id"=>"6507203820"}, {"first_name"=>"Frank J.", "last_name"=>"Schenck", "scopus_author_id"=>"7006167011"}], "year"=>2003, "source"=>"Journal of AOAC International", "identifiers"=>{"pui"=>"36455459", "sgr"=>"0037359650", "pmid"=>"12723926", "scopus"=>"2-s2.0-0037359650", "isbn"=>"1060-3271", "doi"=>"10.1371/journal.pone.0029268", "issn"=>"10603271"}, "id"=>"ebe97fcb-edce-3727-8cdb-de102a704fb7", "abstract"=>"A simple, fast, and inexpensive method for the de- termination of pesticide residues in fruits and veg- etables is introduced. The procedure involves ini- tial single-phase extraction of 10 g sample with 10 mL acetonitrile, followed by liquid–liquid parti- tioning formed by addition of 4 g anhydrous MgSO4 plus 1 g NaCl. Removal of residual water and cleanup are performed simultaneously by us- ing a rapid procedure called dispersive solid-phase extraction (dispersive-SPE), in which 150 mg anhy- drous MgSO4 and 25 mg primary secondary amine (PSA) sorbent are simply mixed with 1mL acetonitrile extract. The dispersive-SPE with PSA effectively removes many polar matrix compo- nents, such as organic acids, certain polar pig- ments, and sugars, to some extent from the food extracts. Gas chromatography/mass spectrometry (GC/MS) is then used for quantitative and confir- matory analysis of GC-amenable pesticides. Re- coveries between 85 and 101%(mostly >95%) and repeatabilities typically <5%have been achieved for a wide range of fortified pesticides, including very polar and basic compounds such as methamidophos, acephate, omethoate, imazalil, and thiabendazole. Using this method, a single chemist can prepare a batch of 6 previously chopped samples in <30 min with approximately $1 (U.S.) of materials per sample.", "link"=>"http://www.mendeley.com/research/fast-easy-multiresidue-method-employing-acetonitrile-extractionpartitioning-dispersive-solidphase-ex", "reader_count"=>357, "reader_count_by_academic_status"=>{"Unspecified"=>19, "Professor > Associate Professor"=>16, "Librarian"=>2, "Researcher"=>52, "Student > Doctoral Student"=>30, "Student > Ph. D. Student"=>88, "Student > Postgraduate"=>17, "Student > Master"=>79, "Other"=>8, "Student > Bachelor"=>34, "Lecturer"=>2, "Lecturer > Senior Lecturer"=>3, "Professor"=>7}, "reader_count_by_user_role"=>{"Unspecified"=>19, "Professor > Associate Professor"=>16, "Librarian"=>2, "Researcher"=>52, "Student > Doctoral Student"=>30, "Student > Ph. D. Student"=>88, "Student > Postgraduate"=>17, "Student > Master"=>79, "Other"=>8, "Student > Bachelor"=>34, "Lecturer"=>2, "Lecturer > Senior Lecturer"=>3, "Professor"=>7}, "reader_count_by_subject_area"=>{"Unspecified"=>37, "Agricultural and Biological Sciences"=>51, "Arts and Humanities"=>1, "Veterinary Science and Veterinary Medicine"=>3, "Chemical Engineering"=>2, "Chemistry"=>170, "Computer Science"=>1, "Earth and Planetary Sciences"=>3, "Engineering"=>11, "Environmental Science"=>46, "Biochemistry, Genetics and Molecular Biology"=>10, "Materials Science"=>3, "Medicine and Dentistry"=>4, "Neuroscience"=>1, "Pharmacology, Toxicology and Pharmaceutical Science"=>12, "Physics and Astronomy"=>1, "Social Sciences"=>1}, "reader_count_by_subdiscipline"=>{"Materials Science"=>{"Materials Science"=>3}, "Medicine and Dentistry"=>{"Medicine and Dentistry"=>4}, "Social Sciences"=>{"Social Sciences"=>1}, "Physics and Astronomy"=>{"Physics and Astronomy"=>1}, "Unspecified"=>{"Unspecified"=>37}, "Environmental Science"=>{"Environmental Science"=>46}, "Pharmacology, Toxicology and Pharmaceutical Science"=>{"Pharmacology, Toxicology and Pharmaceutical Science"=>12}, "Chemical Engineering"=>{"Chemical Engineering"=>2}, "Arts and Humanities"=>{"Arts and Humanities"=>1}, "Engineering"=>{"Engineering"=>11}, "Chemistry"=>{"Chemistry"=>170}, "Neuroscience"=>{"Neuroscience"=>1}, "Earth and Planetary Sciences"=>{"Earth and Planetary Sciences"=>3}, "Agricultural and Biological Sciences"=>{"Agricultural and Biological Sciences"=>51}, "Computer Science"=>{"Computer Science"=>1}, "Biochemistry, Genetics and Molecular Biology"=>{"Biochemistry, Genetics and Molecular Biology"=>10}, "Veterinary Science and Veterinary Medicine"=>{"Veterinary Science and Veterinary Medicine"=>3}}, "reader_count_by_country"=>{"Saudi Arabia"=>1, "Colombia"=>1, "Czech Republic"=>1, "Hungary"=>1, "United States"=>2, "Norway"=>1, "Brazil"=>2, "Portugal"=>1, "Germany"=>1, "Spain"=>2, "India"=>1}, "group_count"=>14}

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Figshare

  • {"files"=>["https://ndownloader.figshare.com/files/696654"], "description"=>"1<p>ND = Not detected.</p>", "links"=>[], "tags"=>["concentrations", "pollen", "removed", "maize", "anthers", "samples", "taken", "hives", "shown", "parts"], "article_id"=>367046, "categories"=>["Biotechnology", "Ecology", "Plant Biology"], "users"=>["Christian H. Krupke", "Greg J. Hunt", "Brian D. Eitzer", "Gladys Andino", "Krispn Given"], "doi"=>["https://dx.doi.org/10.1371/journal.pone.0029268.t003"], "stats"=>{"downloads"=>0, "page_views"=>0, "likes"=>0}, "figshare_url"=>"https://figshare.com/articles/_Pesticide_concentrations_found_in_pollen_removed_from_maize_anthers_at_anthesis_Samples_were_taken_from_the_experimental_field_where_hives_were_placed_All_concentrations_shown_are_expressed_as_parts_per_billion_1_/367046", "title"=>"Pesticide concentrations found in pollen removed from maize anthers at anthesis. Samples were taken from the experimental field where hives were placed. All concentrations shown are expressed as parts per billion.<sup>1</sup>", "pos_in_sequence"=>0, "defined_type"=>3, "published_date"=>"2013-02-20 10:17:06"}
  • {"files"=>["https://ndownloader.figshare.com/files/696695"], "description"=>"1<p>ND  =  Not detected.</p>2<p>**, ***  =  Talc samples taken following planting of treated and untreated sections of experimental fields, respectively, in 2010.</p>", "links"=>[], "tags"=>["concentrations", "talc", "samples", "removed", "planter", "planting", "treated", "untreated", "maize", "shown", "parts"], "article_id"=>367094, "categories"=>["Biotechnology", "Ecology", "Plant Biology"], "users"=>["Christian H. Krupke", "Greg J. Hunt", "Brian D. Eitzer", "Gladys Andino", "Krispn Given"], "doi"=>["https://dx.doi.org/10.1371/journal.pone.0029268.t002"], "stats"=>{"downloads"=>0, "page_views"=>0, "likes"=>0}, "figshare_url"=>"https://figshare.com/articles/_Pesticide_concentrations_found_in_talc_samples_removed_from_planter_following_planting_with_treated_and_untreated_maize_seed_all_concentrations_shown_are_expressed_as_parts_per_million_1_2_/367094", "title"=>"Pesticide concentrations found in talc samples removed from planter following planting with treated and untreated maize seed, all concentrations shown are expressed as parts per million.<sup>1</sup><sup>,</sup><sup>2</sup>", "pos_in_sequence"=>0, "defined_type"=>3, "published_date"=>"2013-02-20 10:17:23"}
  • {"files"=>["https://ndownloader.figshare.com/files/696735"], "description"=>"1<p>ND  =  Not detected.</p>2<p>*  =  Experimental field where hives were placed in 2010.</p>", "links"=>[], "tags"=>["concentrations", "samples", "taken", "fields", "shown", "parts"], "article_id"=>367137, "categories"=>["Biotechnology", "Ecology", "Plant Biology"], "users"=>["Christian H. Krupke", "Greg J. Hunt", "Brian D. Eitzer", "Gladys Andino", "Krispn Given"], "doi"=>["https://dx.doi.org/10.1371/journal.pone.0029268.t001"], "stats"=>{"downloads"=>0, "page_views"=>0, "likes"=>0}, "figshare_url"=>"https://figshare.com/articles/_Pesticide_concentrations_found_in_soil_samples_taken_from_production_fields_surrounding_study_area_all_concentrations_shown_are_expressed_as_parts_per_billion_1_2_/367137", "title"=>"Pesticide concentrations found in soil samples taken from production fields surrounding study area, all concentrations shown are expressed as parts per billion.<sup>1</sup><sup>,</sup><sup>2</sup>", "pos_in_sequence"=>0, "defined_type"=>3, "published_date"=>"2013-02-20 10:17:37"}
  • {"files"=>["https://ndownloader.figshare.com/files/696778"], "description"=>"<p>When two aliquots of the same sample were analyzed the results are expressed as ± the standard deviation of the two analyses.</p>1<p>ND = Not detected.</p>", "links"=>[], "tags"=>["concentrations", "unplanted", "fields", "apiary", "planting", "shown", "parts"], "article_id"=>367181, "categories"=>["Biotechnology", "Ecology", "Plant Biology"], "users"=>["Christian H. Krupke", "Greg J. Hunt", "Brian D. Eitzer", "Gladys Andino", "Krispn Given"], "doi"=>["https://dx.doi.org/10.1371/journal.pone.0029268.t006"], "stats"=>{"downloads"=>0, "page_views"=>0, "likes"=>0}, "figshare_url"=>"https://figshare.com/articles/_Pesticide_concentrations_found_in_unplanted_fields_near_apiary_during_planting_period_in_2011_all_concentrations_shown_are_expressed_as_parts_per_billion_1_/367181", "title"=>"Pesticide concentrations found in unplanted fields near apiary during planting period in 2011, all concentrations shown are expressed as parts per billion.<sup>1</sup>", "pos_in_sequence"=>0, "defined_type"=>3, "published_date"=>"2013-02-20 10:17:49"}
  • {"files"=>["https://ndownloader.figshare.com/files/696812"], "description"=>"<p>When two aliquots of the same sample were analyzed the results are expressed as ± the standard deviation of the two analyses.</p>1<p>ND = Not detected.</p>", "links"=>[], "tags"=>["concentrations", "apiary", "colonies", "planting", "shown", "parts"], "article_id"=>367217, "categories"=>["Biotechnology", "Ecology", "Plant Biology"], "users"=>["Christian H. Krupke", "Greg J. Hunt", "Brian D. Eitzer", "Gladys Andino", "Krispn Given"], "doi"=>["https://dx.doi.org/10.1371/journal.pone.0029268.t005"], "stats"=>{"downloads"=>0, "page_views"=>0, "likes"=>0}, "figshare_url"=>"https://figshare.com/articles/_Pesticide_concentrations_found_in_near_apiary_colonies_during_planting_period_in_2011_all_concentrations_shown_are_expressed_as_parts_per_billion_1_/367217", "title"=>"Pesticide concentrations found in/near apiary colonies during planting period in 2011, all concentrations shown are expressed as parts per billion.<sup>1</sup>", "pos_in_sequence"=>0, "defined_type"=>3, "published_date"=>"2013-02-20 10:18:02"}
  • {"files"=>["https://ndownloader.figshare.com/files/696854"], "description"=>"1<p>ND = Not detected.</p>", "links"=>[], "tags"=>["concentrations", "pollen", "samples", "removed", "returning", "foragers", "hives", "placed", "adjacent", "maize", "fields", "shown", "parts"], "article_id"=>367252, "categories"=>["Biotechnology", "Ecology", "Plant Biology"], "users"=>["Christian H. Krupke", "Greg J. Hunt", "Brian D. Eitzer", "Gladys Andino", "Krispn Given"], "doi"=>["https://dx.doi.org/10.1371/journal.pone.0029268.t004"], "stats"=>{"downloads"=>0, "page_views"=>0, "likes"=>0}, "figshare_url"=>"https://figshare.com/articles/_Pesticide_concentrations_found_in_pollen_samples_removed_from_returning_foragers_of_hives_placed_adjacent_to_maize_fields_at_planting_all_concentrations_shown_are_expressed_as_parts_per_billion_1_/367252", "title"=>"Pesticide concentrations found in pollen samples removed from returning foragers of hives placed adjacent to maize fields at planting, all concentrations shown are expressed as parts per billion.<sup>1</sup>", "pos_in_sequence"=>0, "defined_type"=>3, "published_date"=>"2013-02-20 10:18:13"}

PMC Usage Stats | Further Information

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Relative Metric

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